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Hui Zhang, Xiaohu Xia, Weiyang Li, Jie Zeng, Yunqian Dai, Deren Yang and Younan Xia Facile Synthesis of Five-fold Twinned, Starfish-like Rhodium Nanocrystals by Eliminating Oxidative Etching with a Chloride-Free Precursor Angewandte Chemie International Edition 49

Version of Record online: 23 JUN 2010 | DOI: 10.1002/anie.201002546

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Five-fold twinned, starfish-like Rh nanocrystals consisting of five arms (see TEM) have been synthesized in high yields with the use of [{(CF3COO)2Rh}2] as a precursor to completely eliminate oxidative etching from this system. The as-prepared Rh nanocrystals were shown with great performance as a substrate for SERS.

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