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Dezhi Yang, Lianhuan Han, Yang Yang, Liu-Bin Zhao, Cheng Zong, Yi-Fan Huang, Prof. Dr. Dongping Zhan and Prof. Dr. Zhong-Qun Tian Solid-State Redox Solutions: Microfabrication and Electrochemistry Angewandte Chemie International Edition 50

Article first published online: 26 JUL 2011 | DOI: 10.1002/anie.201103386

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On solid ground: Mix-valent iron hexacyanides (FeIII, FeII, and Prussian blue) can replace NaCl crystal lattice units to form a solid-state solution. A scanning electrochemical microcapillary (SECM) technique has been developed for the controllable microfabrication of the microcrystals. In situ confocal Raman spectra can also be obtained without exposure to any liquid environment. WE=working electrode, RE/CE=reference/counter electrode.

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