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Dr. Aaron J. Rossini, Alexandre Zagdoun, Dr. Moreno Lelli, Dr. Jérôme Canivet, Dr. Sonia Aguado, Dr. Olivier Ouari, Prof. Paul Tordo, Dr. Melanie Rosay, Dr. Werner E. Maas, Prof. Christophe Copéret, Dr. David Farrusseng, Prof. Lyndon Emsley and Dr. Anne Lesage Dynamic Nuclear Polarization Enhanced Solid-State NMR Spectroscopy of Functionalized Metal–Organic Frameworks Angewandte Chemie International Edition 51

Version of Record online: 15 NOV 2011 | DOI: 10.1002/anie.201106030

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A matter of minutes: Dynamic nuclear polarization (DNP) is applied to enhance the signal of solid-state NMR spectra of metal–organic framework (MOF) materials. The signal enhancement enables the acquisition of high-quality 1D 13C solid-state NMR spectra, 2D 1H–13C dipolar HETCOR and 1D 15N solid-state NMR spectra with natural isotopic abundance in experiment times on the order of minutes. MW=microwaves.

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