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Dr. Jianlong Xia and Prof. Ramesh Jasti Synthesis, Characterization, and Crystal Structure of [6]Cycloparaphenylene Angewandte Chemie International Edition 51

Version of Record online: 27 JAN 2012 | DOI: 10.1002/anie.201108167

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Strained: [6]Cycloparaphenylene, a molecule with 97 kcal mol−1 of strain energy, was synthesized. The synthetic strategy relied on two sequential oxidative dearomatization/addition sequences and a final reductive aromatization reaction (see scheme). The optoelectronic properties of [6]cycloparaphenylene were measured, and the analysis of the X-ray crystal structure revealed a linear packing geometry reminiscent of a carbon nanotube.

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