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Takenori Sumi, Dr. Tsuyoshi Saitoh, Keisuke Natsui, Dr. Takashi Yamamoto, Prof. Dr. Mahito Atobe, Prof. Dr. Yasuaki Einaga and Prof. Dr. Shigeru Nishiyama Anodic Oxidation on a Boron-Doped Diamond Electrode Mediated by Methoxy Radicals Angewandte Chemie International Edition 51

Article first published online: 18 APR 2012 | DOI: 10.1002/anie.201200878

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Direct evidence: The existence of methoxy radical species formed during an anodic oxidation in MeOH on a boron-doped diamond (BDD) electrode was confirmed by ESR spectroscopy. Effective production of a neolignan, licarin A, was accomplished by the BDD-mediated anodic oxidation protocol (see picture).

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