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Bin Li, Dr. Yu-Jun Zhao, Yin-Chang Lai and Prof. Teck-Peng Loh Asymmetric Syntheses of 8-Oxabicyclo[3,2,1]octanes: A Cationic Cascade Cyclization Angewandte Chemie International Edition 51

Version of Record online: 2 JUL 2012 | DOI: 10.1002/anie.201202699

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High octane: A novel and practical syntheses of 8-oxabicyclo[3.2.1]octanes using a cationic cascade cyclization reaction has been developed (see scheme; TIPS=triisopropylsilyl). The diastereomer of the cyclization product isolated depends upon whether the acetal or aldehyde substrate is used.

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