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Dr. Hai Fu, Prof. Chao Qin, Prof. Ying Lu, Dr. Zhi-Ming Zhang, Prof. Yang-Guang Li, Prof. Zhong-Min Su, Dr. Wen-Liang Li and Prof. En-Bo Wang An Ionothermal Synthetic Approach to Porous Polyoxometalate-Based Metal–Organic Frameworks Angewandte Chemie International Edition 51

Article first published online: 2 JUL 2012 | DOI: 10.1002/anie.201202994

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Pretty porous POMs: Ionothermal synthesis was applied to prepare porous POM-based open frameworks. The structural integrity remains unchanged until 300 °C; most importantly, the bulky tetrabutylammonium cations within their nanosized channels can be replaced by transition-metal ions through a cation-exchange process, and subsequent gas adsorption measurements confirm their permanent porosity.

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