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Dr. Liang Wang and Prof. Dr. Dirk Menche Concise Synthesis of Acetal-Protected syn 1,3-Diols by a Tandem Hemiacetal Formation/Tsuji–Trost Reaction Angewandte Chemie International Edition 51

Version of Record online: 15 AUG 2012 | DOI: 10.1002/anie.201203911

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Designed, developed, and applied: A novel domino sequence was used for the rapid assembly of acetal-protected syn 1,3-diols. The convergent synthesis of a polyol fragment of the macrolide antibiotic RK-397 demonstrates that this method is suitable for the rapid and stereoselective preparation of polyketide-type diol motifs.

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