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Tadeja Birsa Čelič, Dr. Mojca Rangus, Dr. Károly Lázár, Prof. Venčeslav Kaučič and Prof. Nataša Zabukovec Logar Spectroscopic Evidence for the Structure Directing Role of the Solvent in the Synthesis of Two Iron Carboxylates Angewandte Chemie International Edition 51

Version of Record online: 13 NOV 2012 | DOI: 10.1002/anie.201204573

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Crystal engineering: The synthesis of the known compounds MIL-100(Fe) and MIL-45(Fe) is characterized by spectroscopy. The products are obtained under identical conditions by varying the solvent from pure water to a mixture of water and acetone. The starting solution, the gel, and the final reaction product were characterized by X-ray absorption spectroscopy (see picture).

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