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Dr. M. Carmen Blanco, Dr. Jéssica Cámara, Prof. Dr. M. Concepción Gimeno, Prof. Dr. Antonio Laguna, Prof. Stuart L. James, Dr. M. Cristina Lagunas and Dr. M. Dolores Villacampa Synthesis of Gold–Silver Luminescent Honeycomb Aggregates by Both Solvent-Based and Solvent-Free Methods Angewandte Chemie International Edition 51

Version of Record online: 24 AUG 2012 | DOI: 10.1002/anie.201204859

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Heterometallic clusters with strong luminescence have been synthesized (see picture: Au(C[TRIPLE BOND]CPh)2 yellow-red, Ag2 blue, O red) from the metalloligand unit [Au(C[TRIPLE BOND]CPh)PPh3] (yellow/red bars) by using both standard solvent-based and solvent-free reactions. The aggregates are stabilized only by acetylide–metal or metal–metal interactions, and their nuclearity is controlled through the addition of different donor ligands.

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