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Markus Plois, Waldemar Hujo, Prof. Dr. Stefan Grimme, Christian Schwickert, Dr. Eckhard Bill, Dr. Bas de Bruin, Prof. Dr. Rainer Pöttgen and Prof. Dr. Robert Wolf Open-Shell First-Row Transition-Metal Polyhydride Complexes Based on the fac-[RuH3(PR3)3]− Building Block Angewandte Chemie International Edition 52

Version of Record online: 3 DEC 2012 | DOI: 10.1002/anie.201205209

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High-spin hydrides: A new class of stable paramagnetic polyhydride complexes [M{Ru(μ-H)3(PTol3)3}2] (M=Cr–Ni) with an unprecedented trinuclear arrangement has been synthesized. The high-spin central 3d metal ion is sandwiched between six hydride ligands in a distorted octahedral fashion.

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