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Prof. Dr. Itaru Nakamura, Masashi Okamoto, Yoshinori Sato and Prof. Dr. Masahiro Terada Synthesis of Azepine Derivatives by Rhodium-Catalyzed Tandem 2,3-Rearrangement/Heterocyclization Angewandte Chemie International Edition 51

Article first published online: 31 AUG 2012 | DOI: 10.1002/anie.201205285

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Easy to N-cycle: The efficient synthesis of azepine derivatives was achieved by Rh-catalyzed tandem 2,3-rearrangement involving the heterocyclization of N-allenylnitrone intermediates (see scheme; cod=1,5-cyclooctadiene, tppms=sodium diphenylphosphinobenzene-3-sulfonate).

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