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Teng Wang, Wang Zhou, Hang Yin, Dr. Jun-An Ma and Dr. Ning Jiao Iron-Facilitated Oxidative Dehydrogenative C[BOND]O Bond Formation by Propargylic C sp 3[BOND]H Functionalization Angewandte Chemie International Edition 51

Article first published online: 9 OCT 2012 | DOI: 10.1002/anie.201205779

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Hot couple: Propargyl azides were coupled with carboxylic acids by an iron-catalyzed dehydrogenative C[BOND]O bond formation (see scheme). This method enables propargylic Cmath image[BOND]H functionalization under mild reaction conditions and also may involve the application of the azido moiety as an assisting group in C[BOND]H activation.

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