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Dr. Hiroki Takahashi, Dr. Daniel Lee, Dr. Lionel Dubois, Dr. Michel Bardet, Dr. Sabine Hediger and Dr. Gaël De Paëpe Rapid Natural-Abundance 2D 13C–13C Correlation Spectroscopy Using Dynamic Nuclear Polarization Enhanced Solid-State NMR and Matrix-Free Sample Preparation Angewandte Chemie International Edition 51

Version of Record online: 18 OCT 2012 | DOI: 10.1002/anie.201206102

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Ultra-fast: Substantial solid-state NMR sensitivity can be achieved using dynamic nuclear polarization and matrix-free sample preparation (that is, absence of solvent and cryoprotectant). This method avoids line-broadening, maximizes sample filling factor, and allows natural-abundance 2D 13C–13C dipolar correlation experiments to be carried out in tens of minutes. MW=microwaves.

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