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Yoichi Hoshimoto, Yukari Hayashi, Haruka Suzuki, Dr. Masato Ohashi and Prof. Sensuke Ogoshi Synthesis of Five- and Six-Membered Benzocyclic Ketones through Intramolecular Alkene Hydroacylation Catalyzed by Nickel(0)/N-Heterocyclic Carbenes Angewandte Chemie International Edition 51

Version of Record online: 25 SEP 2012 | DOI: 10.1002/anie.201206186

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Getting some closure: Mechanistic studies supported the participation of an oxanickelacycle complex in the hydroacylation step of the title reaction, which proceeds without decarbonylation even in the absence of well-known chelation assistance by heteroatoms.

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