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Simon P. Curran and Prof. Stephen J. Connon The Thiolate-Catalyzed Intermolecular Crossed Tishchenko Reaction: Highly Chemoselective Coupling of Two Different Aromatic Aldehydes Angewandte Chemie International Edition 51

Version of Record online: 26 SEP 2012 | DOI: 10.1002/anie.201206343

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Crossed products: Ortho-substituted benzaldehydes react with other aromatic aldehydes in a highly selective, atom-economical Tishchenko disproportionation (see scheme) in the presence of a readily prepared, inexpensive thiolate-based catalyst. The methodology is of exceptionally wide scope and exhibits a high functional-group tolerance.

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