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Hui Liu, Chao Dong, Zeguang Zhang, Peiyu Wu and Prof. Dr. Xuefeng Jiang Transition-Metal-Free Aerobic Oxidative Cleavage of C[BOND]C Bonds in α-Hydroxy Ketones and Mechanistic Insight to the Reaction Pathway Angewandte Chemie International Edition 51

Article first published online: 5 NOV 2012 | DOI: 10.1002/anie.201207206

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Clear cut: For the title reaction, O2, the ideal oxidant, was used as the only oxidizing reagent. The dimer intermediate (see scheme) and isotopic labeling control experiments with 18O2 partially disclosed the reaction mechanism.

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