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Dr. Shin-ichi Kawaguchi, Yoshiaki Minamida, Takashi Ohe, Dr. Akihiro Nomoto, Dr. Motohiro Sonoda and Prof. Dr. Akiya Ogawa Synthesis and Properties of Perfluoroalkyl Phosphine Ligands: Photoinduced Reaction of Diphosphines with Perfluoroalkyl Iodides Angewandte Chemie International Edition 52

Article first published online: 4 JAN 2013 | DOI: 10.1002/anie.201207383

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A ‘F'lurry of activity: The title reaction provides a convenient procedure for direct synthesis of perfluoroalkylated phosphines. The synthesized phosphine n-C10F21PPh2 forms a complex with palladium(II) to give 1 and several runs of coupling reactions are attained with n-C10F21PPh2 by using a fluorous/organic biphasic system.

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