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Donghun Kim, Nam Hee Kim and Dr. Sun Hee Kim 34 GHz Pulsed ENDOR Characterization of the Copper Coordination of an Amyloid β Peptide Relevant to Alzheimer’s Disease Angewandte Chemie International Edition 52

Version of Record online: 3 DEC 2012 | DOI: 10.1002/anie.201208108

Thumbnail image of graphical abstract

The copper(II) ion coordination mode of CuII-Aβ(1–16) at physiological pH was characterized by 34 GHz pulsed ENDOR spectroscopy. 1H/2H ENDOR and 14N ENDOR demonstrate the NH2 terminus of aspartic acid is an equatorial ligand of CuII, and 17O ENDOR together with 1H ENDOR suggest that water is an axial ligand (see picture; Cu pink, O red, N blue).

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