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Prof. Dr. Zhiqiang Weng, Weiming He, Chaohuang Chen, Richmond Lee, Davin Tan, Prof. Dr. Zhiping Lai, Dedao Kong, Prof. Dr. Yaofeng Yuan and Prof. Dr. Kuo-Wei Huang An Air-Stable Copper Reagent for Nucleophilic Trifluoromethylthiolation of Aryl Halides Angewandte Chemie International Edition 52

Article first published online: 12 DEC 2012 | DOI: 10.1002/anie.201208432

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A series of copper(I) trifluoromethyl thiolate complexes have been synthesized from the reaction of CuF2 with Me3SiCF3 and S8 (see scheme; Cu red, F green, N blue, S yellow). These air-stable complexes serve as reagents for the efficient conversion of a wide range of aryl halides into the corresponding aryl trifluoromethyl thioethers in excellent yields.

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