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Dr. Xiaoqing Zeng, Dr. Eduard Bernhardt, Dr. Helmut Beckers, Prof. Dr. Klaus Banert, Dr. Manfred Hagedorn and Hailiang Liu Formyl Azide: Properties and Solid-State Structure Angewandte Chemie International Edition 52

Version of Record online: 12 FEB 2013 | DOI: 10.1002/anie.201209288

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The simplest acyl azide, HC(O)N3, has been prepared as the neat substance and characterized by IR and Raman spectroscopy and low-temperature X-ray crystallography (see solid-state structure; C white, H gray, N blue, O red). Photolysis of the azide in CO-doped solid noble-gas matrices furnished the first experimental proof of the elusive parent acyl isocyanate HC(O)NCO.

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