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Xinxin Shao, Xueqiang Wang, Tao Yang, Prof. Dr. Long Lu and Prof. Dr. Qilong Shen An Electrophilic Hypervalent Iodine Reagent for Trifluoromethylthiolation Angewandte Chemie International Edition 52

Version of Record online: 25 JAN 2013 | DOI: 10.1002/anie.201209817

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Sulfur and friends: A new electrophilic hypervalent iodine reagent 1 has been developed for direct trifluoromethylthiolation. A variety of nucleophiles, including β-ketoesters, aldehydes, amides, aryl or vinyl boronic acids, and alkynes, reacted with 1 under mild conditions to give the corresponding trifluoromethylthiolated compounds in good to excellent yields.

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