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Dr. Anne-Marie R. Dechert-Schmitt, Dr. Daniel C. Schmitt and Prof. Michael J. Krische Protecting-Group-Free Diastereoselective C[BOND]C Coupling of 1,3-Glycols and Allyl Acetate through Site-Selective Primary Alcohol Dehydrogenation Angewandte Chemie International Edition 52

Version of Record online: 31 JAN 2013 | DOI: 10.1002/anie.201209863

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Safe from protection! A pronounced kinetic preference for primary alcohol dehydrogenation enables the site-selective iridium catalyzed C[BOND]C coupling of polyols with allyl acetate in the absence of protecting groups, premetallated reagents, chiral auxiliaries, and discrete alcohol-to-aldehyde oxidation.

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