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Dr. Honggen Wang, Bernhard Beiring, Dr. Da-Gang Yu, Dr. Karl D. Collins and Prof. Dr. Frank Glorius [3]Dendralene Synthesis: Rhodium(III)-Catalyzed Alkenyl C[BOND]H Activation and Coupling Reaction with Allenyl Carbinol Carbonate Angewandte Chemie International Edition 52

Version of Record online: 2 OCT 2013 | DOI: 10.1002/anie.201306754

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[3]DendrAl(l)ene! A new synthesis of [3]dendralenes is based on a RhIII-catalyzed alkenyl C[BOND]H activation and coupling reaction with allenyl carbinol carbonates (see scheme; DG=directing group). A variety of [3]dendralenes with diverse substitution patterns are accessible with good efficiency. The reaction is highly stereoselective and compatible with different directing groups and numerous functional groups.

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