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Jun Yi, Xi Lu, Yan-Yan Sun, Bin Xiao and Prof. Lei Liu Nickel-Catalyzed Sonogashira Reactions of Non-activated Secondary Alkyl Bromides and Iodides Angewandte Chemie International Edition 52

Article first published online: 2 OCT 2013 | DOI: 10.1002/anie.201307069

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A nicked reaction: The title reaction of terminal alkynes with non-activated secondary alkyl iodides and bromides was accomplished for the first time. This reaction provides a new and practical approach for the synthesis of substituted alkynes (see scheme; cod=cyclo-1,5-octadiene).

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