Dr. Waka Nakanishi, Yusuke Shimada and Prof. Hiroyuki Isobe Structural Fluctuation of Disilanyl Double-Pillared Bisheteroarenes Chemistry – An Asian Journal 8
One, two, three: Three congeners of disilanyl double-pillared bisheteroarenes have been synthesized by a concise one-pot synthetic procedure. The step-like structures of the silacyclophanes were revealed by X-ray crystallographic analysis. The step-like structures, however, fluctuated in a solution phase in the presence of steric congestions, and the dynamics were disclosed by NMR spectroscopy.
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