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Arghya Sadhukhan, Dr. Manoj K. Choudhary, Dr. Noor-ul H. Khan, Dr. Rukhsana I. Kureshy, Dr. Sayed H. R. Abdi and Hari C. Bajaj Asymmetric Cyanoethoxy Carbonylation Reaction of Aldehydes Catalyzed by a TiIV Macrocyclic Complex: An Efficient Synthetic Protocol for β-Blocker and α1-Adrenergic Receptor Agonists ChemCatChem 5

Article first published online: 9 JAN 2013 | DOI: 10.1002/cctc.201200617

Thumbnail image of graphical abstract

A crown of titanium: A new class of chiral macrocyclic TiIV–salen complexes are efficient, recyclable, and scalable catalysts for the asymmetric addition of ethyl cyanoformate to aldehydes, which is useful for the synthesis of bioactive compounds. The figure shows the best-performing ligand with two salen units linked flexibly in a crown ether-like motif.

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