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Shintaro Itagaki, Dr. Keigo Kamata, Dr. Kazuya Yamaguchi and Prof. Dr. Noritaka Mizuno A Monovacant Lacunary Silicotungstate as an Efficient Heterogeneous Catalyst for Dehydration of Primary Amides to Nitriles ChemCatChem 5

Article first published online: 15 APR 2013 | DOI: 10.1002/cctc.201300063

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Acting up with nitriles: A monovacant lacunary silicotungstate, TBA4[α-H4SiW11O39] (I) could act as an efficient heterogeneous catalyst for dehydration of primary amides. Various kinds of primary amides, including benzylic, double bond-containing, heteroaromatic, and aliphatic could be converted into the corresponding nitriles in moderate to excellent yields.

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