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Prof. Dr. Qiufeng Huang, Shaojia Ke, Lin Qiu, Xiaofeng Zhang and Prof. Dr. Shen Lin Palladium(II)/Polyoxometalate-Catalyzed Direct Alkenylation of Benzofurans under Atmospheric Dioxygen ChemCatChem 6

Article first published online: 16 APR 2014 | DOI: 10.1002/cctc.201400091

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A tolerant POM: The efficient and selective direct alkenylation of benzofurans is achieved by using palladium acetate combined with 11-molybdovanadophosphoric acid. The transformation is performed under an atmosphere of dioxygen. Functional groups such as ethoxy, cyano, chloro, bromo, and ester are tolerated under the reaction conditions, and N-acetylglycine (Ac-Gly-OH) appears to be an effective additive for this reaction. 1 atm=101.3 kPa.

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