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Dr. Alan A. Wilson, Armando Garcia, Dr. Sylvain Houle, Dr. Oleg Sadovski and Dr. Neil Vasdev Synthesis and Application of Isocyanates Radiolabeled with Carbon-11 Chemistry - A European Journal 17

Version of Record online: 12 NOV 2010 | DOI: 10.1002/chem.201002345

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Who needs phosgene anyway? Carbon-11 labeled isocyanates can be efficiently prepared by dehydration of [11C]carbamate salts, which in turn are easily formed from [11C]CO2 and amines in the presence of a CO2 fixation agent. The [11C]isocyanates are useful radiosynthons for the synthesis of a variety of [carbonyl-11C]-labeled asymmetrical ureas and carbamate esters (see scheme).

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