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Martins S. Oderinde and Prof. Michael G. Organ Pronounced Solvent Effect on the Hydrostannylation of Propargylic Alcohol Derivatives with nBu3SnH/Et3B at Room Temperature Chemistry - A European Journal 19

Version of Record online: 10 JAN 2013 | DOI: 10.1002/chem.201203405

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The solvent is key: A general protocol is described for the hydrostannylation of propargyl alcohol derivatives at room temperature using Et3B/O2 as the promoter (see scheme). Rate and mechanistic studies point to a different autoxidation product of Et3B in THF than is observed in benzene, the typical solvent.

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