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Haizhen Zhang and Fajun Nan Synthesis toward the Lindenane-type Sesquiterpenoid Monomer of Chlorahololide A Chinese Journal of Chemistry 31

Article first published online: 11 DEC 2012 | DOI: 10.1002/cjoc.201200695

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Starting from alcohol (2), and on the basis of Yamamoto rearrangement, intramolecular cyclopropanation reaction, 1,3-dipolar cyclization, and intramolecular Heck reaction, the Lindenane-type sesquiterpenoid fragement (20) of Chlorahololide A (1) has been synthesized in a linear sequence of 21 steps and an overall yield of 1.8%. The flexible synthetic route could generate further natural products of the Chloranthaceae family.

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