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Alejandra M. Ricci, Dr. Lucila P. Méndez De Leo, Prof. Federico J. Williams and Prof. Ernesto J. Calvo Some Evidence for the Formation of an Azo Bond during the Electroreduction of Diazonium Salts on Au Substrates ChemPhysChem 13

Version of Record online: 23 MAR 2012 | DOI: 10.1002/cphc.201100882

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Azo tether: Molecular films obtained by electrochemical reduction of diazonium tetrafluoroborate salts of 4-carboxy benzene and 4-amino-(2,3,5,6-tetrafluoro)-carboxy benzene on Au substrates are studied by a combination of X-ray photoelectron and polarization-modulation infrared reflection absorption spectroscopy. The spectroscopic evidence demonstrates the formation of N[DOUBLE BOND]N bonds tethering the complexes to Au (see picture).

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