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Dr. Bruno Grignard, Prof. Bernard Gilbert, Cedric Malherbe, Prof. Christine Jérôme and Dr. Christophe Detrembleur Online Monitoring of Heterogeneous Polymerizations in Supercritical Carbon Dioxide by Raman Spectroscopy ChemPhysChem 13

Article first published online: 14 JUN 2012 | DOI: 10.1002/cphc.201200373

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A novel setup is described to monitor the kinetics of homogeneous and heterogeneous reactions online using Raman spectroscopy under high pressure. The arrangement is based on a high-pressure reactor equipped with a sapphire window in combination with a mobile probe that allows the collection of the back-scattered Raman signal at 360°.

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