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Dr. Charles Esnault, Dr. Nicolas Delorme, Prof. Guy Louarn and Prof. Jean-François Pilard One-Pot in Situ Mixed Film Formation by Azo Coupling and Diazonium Salt Electrografting ChemPhysChem 14

Version of Record online: 23 APR 2013 | DOI: 10.1002/cphc.201300007

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So simple: The in situ synthesis of an aryldiazonium salt and an azo-aryldiazonium salt by azo coupling from sulfanilic acid and aniline is reported. Formation of a mixed organic layer is monitored by cyclic voltammetry and atomic force microscopy. A compact mixed layer is obtained with a global roughness of 0.4 nm and 10–15 % vertical extension in the range 1.5–6 nm.

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