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Prof. Kay Saalwächter Robust NMR Approaches for the Determination of Homonuclear Dipole–Dipole Coupling Constants in Studies of Solid Materials and Biomolecules ChemPhysChem 14

Version of Record online: 10 JUN 2013 | DOI: 10.1002/cphc.201300254

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Between the poles: The use of different strategies to account for intensity loss in homonuclear double-quantum nuclear magnetic resonance experiments for dipolar coupling quantification is discussed, stressing the use of intensity normalization through a separately measured reference intensity. Similarities to the heteronuclear case of rotational-echo double-resonance experiments are pointed out, and comparisons are made with alternative constant-time approaches.

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