Ricardo Kurz, Marcio Fernando Cobo, Prof. Dr. Eduardo Ribeiro de Azevedo, Dr. Michael Sommer, Dr. André Wicklein, Prof. Dr. Mukundan Thelakkat, Dr. Günter Hempel and Prof. Dr. Kay Saalwächter Avoiding Bias Effects in NMR Experiments for Heteronuclear Dipole–Dipole Coupling Determinations: Principles and Application to Organic Semiconductor Materials ChemPhysChem 14
Dippy curves! Distortions of 13C-detected dipolar chemical-shift correlation (DIPSHIFT) modulation curves arising from a nonisotropic magnetization distribution after short cross-polarization times are demonstrated and explained by theoretical and experimental approaches. The problem is of general importance and practical solutions as well as an application are presented.
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