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Dr. Nicola Castellucci, Prof. Giuseppe Falini, Dr. Lorenzo Milli, Prof. Magda Monari, Prof. Sergio Abbate, Prof. Giovanna Longhi, Dr. Ettore Castiglioni, Dr. Giuseppe Mazzeo and Prof. Claudia Tomasini Solid-State Properties and Vibrational Circular Dichroism Spectroscopy in Solution of Hybrid Foldamers Stereoisomeric Mixtures ChemPlusChem 79

Article first published online: 8 NOV 2013 | DOI: 10.1002/cplu.201300306

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Two wrongs make a right: A 1:1 mixture of Boc-(L-Phe-L-Oxd)2-OBn and Boc-L-Phe-L-Oxd-D-Phe-L-Phe-OBn (Boc = tert-butyloxycarbonyl; L-Oxd=trans-(4S,5R)-4-carboxy 5-methyloxazolidin-2-one, Bn=benzyloxycarbonyl; see picture) form single crystals suitable for X-ray diffraction, whereas the two pure oligomers do not. This mixture forms crystals, fibers and globules, depending on the solvent.

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