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Tony Szuppa, Dr. Achim Stolle, Prof. Bernd Ondruschka and Wieland Hopfe An Alternative Solvent-Free Synthesis of Nopinone under Ball-Milling Conditions: Investigation of Reaction Parameters ChemSusChem 3

Article first published online: 24 AUG 2010 | DOI: 10.1002/cssc.201000122

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A solvent-free method for the synthesis of nopinone from the renewable monoterpene β-pinene in a ball mill is evaluated. The envisioned synthesis pathway uses non-hazardous reagents and is performed under ambient, non-inert reaction conditions. The influence of both technical and chemical reaction parameters on conversion, selectivity, and yield is assessed.

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