Dr. Joseph T. Hill-Cousins, Dr. Jekaterina Kuleshova, Robert A. Green, Dr. Peter R. Birkin, Prof. Derek Pletcher, Toby J. Underwood, Dr. Stuart G. Leach and Prof. Richard C. D. Brown TEMPO-Mediated Electrooxidation of Primary and Secondary Alcohols in a Microfluidic Electrolytic Cell ChemSusChem 5
TEMPO and no salt in sight: A general procedure for the 2,2,6,6-tetramethylpiperidine-1-oxyl (TEMPO)-mediated electrooxidation of primary and secondary alcohols modified for application in a microfluidic electrolytic cell is described. The reaction is performed at ambient temperature in buffered aqueous tBuOH without additional electrolyte.
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