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Suresh Raju, Dr. Johann T. B. H. Jastrzebski, Dr. Martin Lutz and Prof. Dr. Robertus J. M. Klein Gebbink Catalytic Deoxydehydration of Diols to Olefins by using a Bulky Cyclopentadiene-based Trioxorhenium Catalyst ChemSusChem 6

Version of Record online: 10 JUL 2013 | DOI: 10.1002/cssc.201300364

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In the bulk of it: Bulky 1,2,4-tri(tert-butyl)cyclopentadienyl trioxorhenium was studied as a catalyst for the deoxydehydration of different vicinal diols. Under optimised conditions, a variety of vicinal diols were converted into olefins in good to excellent yields, and with minimal olefin isomerisation. Biomass-derived polyols were also converted into their corresponding olefinic products.

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