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Dr. Kirsten M. Ø. Jensen, Dr. Christoffer Tyrsted, Dr. Martin Bremholm and Prof. Dr. Bo B. Iversen In Situ Studies of Solvothermal Synthesis of Energy Materials ChemSusChem 7

Article first published online: 5 MAR 2014 | DOI: 10.1002/cssc.201301042

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In the thick of it: In situ X-ray and neutron studies of solvothermal and hydrothermal reactions can yield new information on the synthesis of energy material and map the structure–synthesis relationship. Various approaches to in situ powder diffraction and total scattering are reviewed. This review discusses experimental methods as well as strategies for data analysis and highlights the chemical insights that can be obtained from in situ experiments.

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