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Michael Becker, Raoul Naumann d'Alnoncourt, Kevin Kähler, Jelena Sekulic, Roland A. Fischer and Martin Muhler The Synthesis of Highly Loaded Cu/Al2O3 and Cu/ZnO/Al2O3 Catalysts by the Two-Step CVD of CuIIdiethylamino-2-propoxide in a Fluidized-Bed Reactor Chemical Vapor Deposition 16

Version of Record online: 22 MAR 2010 | DOI: 10.1002/cvde.200906808

Highly loaded copper catalysts supported on alumina were synthesized applying the cyclic two-step chemical vapor deposition of the precursor copper(II)diethylamino-2-propoxide in a fluidized-bed reactor. Copper/zinc oxide/alumina composites were synthesized by either the CVD of the precursor bis[bis(trimethylsilyl)amido]zinc on Cu/Al2O3, or by the CVD of the Cu precursor on Zn-pretreated alumina. The turn-over frequencies in methanol synthesis of these Cu/ZnO/Al2O3 catalysts were higher than that of a commercial ternary catalyst.

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