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Ana I. S. Neves, Isabel C. Santos, Laura C. J. Pereira, Concepció Rovira, Eliseo Ruiz, Dulce Belo and Manuel Almeida Ni-2,3-thiophenedithiolate Anions in New Architectures: An In-Line Mixed-Valence Ni Dithiolene (Ni4–S12) Cluster European Journal of Inorganic Chemistry 2011

Article first published online: 15 SEP 2011 | DOI: 10.1002/ejic.201100797

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[K(15-crown-5)2]2[Ni4(α-tpdt)6] was prepared by oxidation of the dianionic [Ni(α-tpdt)2]2– complex and was characterised by X-ray crystallography. This compound constitutes an unprecedented example of an in-line mixed-valence Ni4 dithiolene (Ni4S12) cluster.

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