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Szymon Z. Konieczka, Alexander Himmelspach, Michael Hailmann and Maik Finze Synthesis, Characterization, and Selected Properties of 7- and 12-Ammoniocarba-closo-dodecaboranes European Journal of Inorganic Chemistry 2013

Version of Record online: 9 NOV 2012 | DOI: 10.1002/ejic.201200969

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Carba-closo-dodecaboron clusters with an ammonio substituent bonded to the 7- or 12-position of the cluster were synthesized by a microwave-assisted Buchwald–Hartwig cross-coupling reaction. Selected spectroscopic and chemical properties of 12-H3N-closo-1-CB11H11 and 7-H3N-12-Hal-closo-1-CB11H10 (Hal = F, Cl) are reported and compared to data derived from theoretical calculations.

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