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Ming Li, Deng-Bing Li, Jing Pan, Jian-Chao Lin and Guang-Hai Li Selective Synthesis of Vanadium Oxides and Investigation of the Thermochromic Properties of VO2 by Infrared Spectroscopy European Journal of Inorganic Chemistry 2013

Article first published online: 17 DEC 2012 | DOI: 10.1002/ejic.201201118

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An approach combing sol–gel and hydrothermal methods is described for the selective synthesis of vanadium oxides based on the phase evolution sequence V2O5 [RIGHTWARDS ARROW] V3O7·H2O [RIGHTWARDS ARROW] VO2 (B) [RIGHTWARDS ARROW] VO2 (A) [RIGHTWARDS ARROW] VO2 (M). A mechanism for the formation of the vanadium oxides based on the oriented attachment (OA) growth model is proposed. The highly pure VO2 (M) phase shows prominent infrared modulation properties.

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