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Lubin Ni, Bernhard Spingler, Stephen Weyeneth and Greta R. Patzke Trilacunary Keggin-Type POMs as Versatile Building Blocks for Lanthanoid Silicotungstates European Journal of Inorganic Chemistry 2013

Version of Record online: 19 DEC 2012 | DOI: 10.1002/ejic.201201186

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The structure-directing potential of lanthanoid cations for controlling POM architectures is combined with the versatile {SiW9O34} precursor. Depending on the synthetic conditions, {SiW9O34} can be transformed into Keggin-type sandwich compounds or into 2D/3D arrangements of the open Wells–Dawson silicotungstate {Si2W18O66}. This amplifies the linker functions of mid-lanthanoid cations in POM design.

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