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Ties J. Korstanje, Emma Folkertsma, Martin Lutz, Johann T. B. H. Jastrzebski and Robertus J. M. Klein Gebbink Synthesis, Characterization, and Catalytic Behavior of Dioxomolybdenum Complexes Bearing AcAc-Type Ligands European Journal of Inorganic Chemistry 2013

Version of Record online: 8 FEB 2013 | DOI: 10.1002/ejic.201201350

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A series of [MoO2(acac′)2] complexes have been synthesized from sodium molybdate and the desired ligand in good yields and characterized by various spectroscopic techniques and X-ray diffraction. These complexes were found to catalyze the dehydration of various alcohols, from benzylic to aliphatic, allylic and homoallylic, to yield the corresponding olefin.

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