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Masaki Nishio, Shinnosuke Inami and Yoshihito Hayashi Early-Lanthanide Complexes with All-Inorganic Macrocyclic Polyoxovanadate Ligands European Journal of Inorganic Chemistry 2013

Version of Record online: 29 JAN 2013 | DOI: 10.1002/ejic.201201435

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Complexes [LnVnO3n](n–3)– (Ln = LaIII, n = 10; Ln = CeIII, n = 9 or 10; Ln = PrIII, n = 9) with all-inorganic crown ether type polyoxovanadate ligands were synthesized and characterized by single-crystal X-ray diffraction studies. Site exchange of the coordinated and uncoordinated VO4 units in the heteropolyoxometalate frameworks was observed through variable-temperature 51V NMR spectroscopic studies.

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