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Gael Baldissin, Neil M. Boag, Chiu C. Tang and Daniel J. Bull Synthesis of Pure Lithium Amide Nanoparticles European Journal of Inorganic Chemistry 2013

Article first published online: 8 MAR 2013 | DOI: 10.1002/ejic.201201535

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Pure lithium amide can be synthesised efficiently by deprotonation of ammonia with n-butyl lithium. In comparison to commercial samples, the lithium amide produced is a pure, free-flowing powder that quantitatively generates lithium imide at 600 K. The methodology readily affords the production of pure lithium amide and imide and their deuterated analogues at both bench-top and commercial scale.

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