Gael Baldissin, Neil M. Boag, Chiu C. Tang and Daniel J. Bull Synthesis of Pure Lithium Amide Nanoparticles European Journal of Inorganic Chemistry 2013
Pure lithium amide can be synthesised efficiently by deprotonation of ammonia with n-butyl lithium. In comparison to commercial samples, the lithium amide produced is a pure, free-flowing powder that quantitatively generates lithium imide at 600 K. The methodology readily affords the production of pure lithium amide and imide and their deuterated analogues at both bench-top and commercial scale.
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